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Table 1 Ion transitions and instrumental parameters for their LC–MS/MS quantification in MRM mode

From: Mother root of Aconitum carmichaelii Debeaux exerts antinociceptive effect in Complete Freund’s Adjuvant-induced mice: roles of dynorphin/kappa-opioid system and transient receptor potential vanilloid type-1 ion channel

Sample Ion mode MRM CV CE LOQ LOD
Benzoylmesaconine + 590.33 > 77.02 52 78 2.1 0.73
Aconitine + 646.39 > 586.34 50 34 1.9 0.6
Mesantine + 632.33 > 105.04 42 56 2.2 0.9
Benzoylhypacoitine + 574.32 > 542.35 46 34 1.8 0.6
Benzoylaconitine + 604.41 > 105.04 58 54 4.3 1.7
Hypaconitine + 616.36 > 556.31 42 32 1.9 0.61
Reserpine(is) + 609.33 > 174.07 40 42
  1. IS internal standard, CE collision energy (eV), CV cone voltage (V), MRM specific mass transition, LOQ limit of quantification (ng/ml), LOD limit of detection (ng/ml)